Abstract:
A new synthesis of l,6-trimethylene-5-cyano-2-mercapto-l,3,2-diazaphosphorine-2,4-dithione (by treatment of enamines with phosphorus pentasulfide in the presence of pyridine) has been developed and some of its reactions are discussed.
Document Type:
Article
Language: English
Citation:
D. B. Nilov, A. V. Kadushkin, N. P. Solov'eva, A. L. Sedov, V. G. Granik, “Interaction of P2S5–pyridine with enamines. Synthesis and reactions of l,6-trimethylene-5-cyano-2-mercapto-l,3,2-diazaphosphorine-2-thione”, Mendeleev Commun., 6:5 (1996), 191–193
Linking options:
https://www.mathnet.ru/eng/mendc4974
https://www.mathnet.ru/eng/mendc/v6/i5/p191
This publication is cited in the following 12 articles:
V. V. Dotsenko, V. A. Dushenko, N. A. Aksenov, I. V. Aksenova, E. E. Netreba, “Unexpected Result of Thiophosphorylation of 6-Aminopyrano[2,3-c]pyrazole-5-carbonitrile Derivative”, Russ J Gen Chem, 89:9 (2019), 1752
Victor V. Dotsenko, Vladimir A. Dushenko, Nikolai A. Aksenov, Inna V. Aksenova, Evgeniy E. Netreba, 22nd International Electronic Conference on Synthetic Organic Chemistry, 2018, 26
Tarik E. Ali, Mohamed A. Assiri, Somaia M. Abdel-Kariem, Ibrahim S. Yahia, “Facile synthesis of novel 6-methyl-5-phenyl-2-sulfido-1,2,3,5-tetrahydro-4H[1,2] oxazolo[4′,5′:5,6]pyrano[2,3-d][1,3,2]diazaphosphinines”, Journal of Sulfur Chemistry, 39:5 (2018), 472
Tarik E. Ali, Mamdouh M. Ali, Somaia M. Abdel-Kariem, Marwa M. Ahmed, “Reaction of 2-cyano[(4-oxo-4H-chromen-3-yl)methylidene]acetohydrazide with phosphorus reagents: Synthesis and evaluation of anticancer activities of some novel 1,2-azaphospholes, 1,2,3-diazaphospholidine, and 1,3,2-diaza-phosphinanes bearing a chromone ring”, Synthetic Communications, 47:16 (2017), 1458
Sarra Hichri, Raoudha Abderrahim, “A Convenient Synthesis of 1,3,2-Benzodiazaphophorine-2-oxide”, Phosphorus, Sulfur, and Silicon and the Related Elements, 190:1 (2015), 29
M.-G. A. Shvekhgeimer, “Five-, Six-, and Seven-membered Lactim Ethers. Methods of Synthesis and Chemical Properties. (Review)”, Chem Heterocycl Compd, 41:5 (2005), 551
D. B. Nilov, V. G. Granik, “Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives”, Mendeleev Commun., 13:2 (2003), 78–79
Gottfried Maerkl, Peter Kreitmeier, Phosphorus-Carbon Heterocyclic Chemistry, 2001, 535
Vladimir G. Granik, Vadim A. Makarov, Cyril Párkányi, Advances in Heterocyclic Chemistry, 72, Advances in Heterocyclic Chemistry Volume 72, 1998, 283
D. B. Nilov, N. P. Solov'eva, I. S. Nikolaeva, V. V. Peters, L. Yu. Krylova, T. A. Gus'kova, V. G. Granik, “Synthesis and antiviral activity of pyrazolo[3,4-d]-1,3,2-diazaphosphorins”, Pharm Chem J, 32:7 (1998), 358
D. B. NILOV, A. V. KADUSHKIN, N. P. SOLOV'EVA, A. L. SEDOV, V. G. GRANIK, “ChemInform Abstract: Interaction of P2S5‐Pyridine with Enamines. Synthesis and Reactions of 1,6‐Trimethylene‐5‐cyano‐2‐mercapto‐1,3,2‐diazaphosphorine‐2‐thione.”, ChemInform, 28:9 (1997)
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