Аннотация:
The synthesis of the first co-crystals among 4,5-dihydroxy-4,5-diphenylimidazolidin-2-ones (4,5-dihydroxyimidazolidine- 2-thione + 5-hydroxy-4-methoxy-4,5-diphenyl-1,3-diethylimidazolidine-2-thione) and of the cis isomer of 1,3-diethyl-4,5-dihydroxy- 4,5-diphenylimidazolidine-2-thione through the regiospecific condensation of 1,3-diethylthiourea with 1,2-dioxo-1,2-diphenylethane was implemented; the structure was ascertained by single crystal X-ray diffraction and X-ray phase analysis.
Тип публикации:
Статья
Язык публикации: английский
Образец цитирования:
V. V. Baranov, Yu. V. Nelyubina, A. A. Korlyukov, A. N. Kravchenko, “Co-crystals in the series of 4,5-dihydroxy- 4,5-diphenylimidazolidine-2-thiones”, Mendeleev Commun., 19:4 (2009), 211–213
Образцы ссылок на эту страницу:
https://www.mathnet.ru/rus/mendc3173
https://www.mathnet.ru/rus/mendc/v19/i4/p211
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Н. Н. Махова, Л. И. Беленький, Г. А. Газиева, И. Л. Далингер, Л. С. Константинова, В. В. Кузнецов, А. Н. Кравченко, М. М. Краюшкин, О. А. Ракитин, А. М. Старосотников, Л. Л. Ферштат, С. А. Шевелев, В. З. Ширинян, В. Н. Яровенко, “Прогресс в химии азот-, кислород- и серасодержащих гетероциклических систем”, Усп. хим., 89:1 (2020), 55–124; N. N. Makhova, L. I. Belen'kii, G. A. Gazieva, I. L. Dalinger, L. S. Konstantinova, V. V. Kuznetsov, A. N. Kravchenko, M. M. Krayushkin, O. A. Rakitin, A. M. Starosotnikov, L. L. Fershtat, S. A. Shevelev, V. Z. Shirinian, V. N. Yarovenko, “Progress in the chemistry of nitrogen-, oxygen- and sulfur-containing heterocyclic systems”, Russian Chem. Reviews, 89:1 (2020), 55–124
Mohamed Ali Tabarki, Rafâa Besbes, “Selective synthesis of imidazolidine-2-thiones via ring expansion of aziridine-2-carboxylates with isothiocyanates”, Tetrahedron Letters, 57:34 (2016), 3832
Vivek Gupta, Vedhagiri Karthik, Ganapathi Anantharaman, “Labile dioxy-functionalised zwitterionic imidazolinium salt: access to zwitterionic and neutral imidazolidin-2-ylidene derivatives and π-acceptor properties of imidazolidine-2-selones”, RSC Adv., 5:107 (2015), 87888
V. V. Baranov, A. N. Kravchenko, Yu. V. Nelyubina, “Synthesis of new ring-fused thiocarbamates by condensation of 2-thioxo-and 2-oxo-1,3-dialkyl-4,5-dihydroxy-4,5-diphenylimidazolidines with KSCN”, Mendeleev Commun., 24:2 (2014), 105–107
A. N. Kravchenko, V. V. Baranov, Yu. V. Nelyubina, G. A. Gazieva, I. V. Svitan'ko, “Diastereoselective synthesis of 4,5-dihydroxyimidazolidin-2-ones (-thiones) and their structure”, Russ Chem Bull, 61:1 (2012), 64
G. A. Gazieva, V. V. Baranov, A. N. Kravchenko, N. N. Makhova, “α-Thioureidoalkylation of functionally substituted ureas: II. Synthesis of thio analogs of N-hydroxyalkyl-1,5-diphenylglycolurils”, Russ J Org Chem, 47:10 (2011), 1572
V. V. Baranov, G. A. Gazieva, Yu. V. Nelyubina, A. N. Kravchenko, N. N. Makhova, “α-Thioureidoalkylation of functionally substituted ureas: I. Tandem cyclization and esterification in reactions of N-(carboxyalkyl)ureas with 1,3-dialkyl-4,5-dihydroxy-4,5-diphenylimidazolidine-2-thiones in alcohols”, Russ J Org Chem, 47:10 (2011), 1564