aDepartment of Chemistry, Southwest University of Science and Technology, Mianyang, P.R. China bXi'an Modern Chemistry Research Institute, Xi'an, P.R. China cSchool of Materials Science and Engineering, Southwest University of Science and Technology, Mianyang, P.R. China
Аннотация:
The nitrogen–nitrogen double bond between two molecules of 3,5-diamino-1H-1,2,4-triazole is successfully constructed using a one-step electrochemical coupling method. The oxidation occurs selectively when the electrochemical parameters are properly adjusted to provide a yield of 45.77%. Subsequently, the oxidative coupling of this substrate with electrochemically generated hydroxy nickel oxide or sodium hypochlorite is verified.
Ключевые слова:
electrochemical synthesis, conjugation reaction, active site, clean and efficient, triazoles, azo compounds, voltage control.
Образец цитирования:
M. Xie, J. Gong, J. Zhou, J. Wang, Yu. Cao, T. Zhou, Ya. Dai, “Green coupling of 3,5-diamino-1H-1,2,4-triazole into the azo compound”, Mendeleev Commun., 33:5 (2023), 717–720
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