Abstract:
A versatile single-step procedure was proposed for the synthesis of the title compounds by the interaction of equimolar amounts of aliphatic carbonyl compounds, primary aliphatic amines and N-chloroalkylamines in an aprotic organic solvent in the presence of potassium carbonate.
Document Type:
Article
Language: English
Citation:
N. N. Makhova, A. N. Mikhailyuk, V. V. Kuznetsov, S. A. Kutepov, P. A. Belyakov, “Effective synthesis of 1,2-di-, 1,2,3-tri-, 1,2,3,3-tetraalkyldiaziridines and 1,5-diazabicyclo[3.1.0]hexanes”, Mendeleev Commun., 10:5 (2000), 182–185
Linking options:
https://www.mathnet.ru/eng/mendc4447
https://www.mathnet.ru/eng/mendc/v10/i5/p182
This publication is cited in the following 12 articles:
Vladimir V. Kuznetsov, Ilya I. Marochkin, Alexander S. Goloveshkin, Nina N. Makhova, Igor F. Shishkov, “Comparable study of the structure of 1,2-bis(2-acetamidoethyl) diaziridine and 3,3-diethyldiaziridine with structures of related compounds by X-ray diffraction analysis and quantum chemical calculations”, Struct Chem, 28:4 (2017), 1211
Kerstin Zawatzky, Matthias Kamuf, Oliver Trapp, “Chiral 1,2‐Dialkenyl Diaziridines: Synthesis, Enantioselective Separation, and Nitrogen Inversion Barriers”, Chirality, 27:2 (2015), 156
V. V. Kuznetsov, V. V. Seregin, D. V. Khakimov, T. S. Pivina, M. D. Vedenyapina, A. A. Vedenyapin, N. N. Makhova, “The study of the formation mechanism of 1,2,3-trialkyldiaziridines by kinetic and quantum chemistry methods”, Russ Chem Bull, 63:9 (2014), 2000
Vera Yu. Petukhova, Leonid L. Fershtat, Vadim V. Kachala, Vladimir V. Kuznetsov, Dmitriy V. Khakimov, Tatyana S. Pivina, Nina N. Makhova, “Reaction of 1,2‐Dialkyldiaziridines and 1,2,3‐Trialkyldiaziridines with Methyl Propiolate in Ionic Liquids and in Organic Solvents”, Journal of Heterocyclic Chem, 50:2 (2013), 326
Yu. S. Syroeshkina, V. V. Kuznetsov, K. A. Lyssenko, N. N. Makhova, “Insertion of carbon disulfide and the nitrile group into the diaziridine ring of 6-aryl-1,5-diazabicyclo[3.1.0]hexanes in ionic liquids catalyzed by BF3 · Et2O”, Russ Chem Bull, 58:2 (2009), 366
A. V. Shevtsov, V. V. Kuznetsov, S. I. Molotov, K. A. Lyssenko, N. N. Makhova, “Synthesis of 4-aroyl-1,2,4-triazolidin-3-ones via ring extension in reactions of 1,2-di-and 1,2,3,3-tetraalkyldiaziridines with aroyl isocyanates”, Russ Chem Bull, 55:3 (2006), 554
A. V. Shevtsov, V. V. Kuznetsov, K. A. Lyssenko, P. A. Belyakov, N. N. Makhova, “Synthesis of 4-benzoyl-1,2,6-trialkyl-1,2,4,6-tetrazepane-5-thiones by the interaction of 1,2-dialkyldiaziridines with benzoyl isothiocyanate in ionic liquids”, Mendeleev Commun., 16:4 (2006), 218–220
V. V. Kuznetsov, N. N. Makhova, D. E. Dmitriev, V. V. Seregin, “Syntheses of 1,2-di- and 1,2,3-trialkyldiaziridines”, Mendeleev Commun., 15:3 (2005), 116–118
Nina N. Makhova, Anatolii N. Mikhailyuk, Vladimir V. Kuznetsov, Sergei A. Kutepov, Pavel A. Belyakov, “ChemInform Abstract: Effective Synthesis of 1,2‐Di‐, 1,2,3‐Tri‐, 1,2,3,3‐Tetraalkyldiaziridines and 1,5‐Diazabicyclo[3.1.0]hexanes.”, ChemInform, 32:8 (2001)
N. N. Makhova, N. G. Kamalova, Yu. A. Strelenko, “Synthesis of the first representatives of 3-ethynyldiaziridines”, Mendeleev Commun., 11:6 (2001), 227–229
A. V. Shevtsov, V. Yu. Petukhova, S. A. Kutepov, V. V. Kuznetsov, N. N. Makhova, N. E. Kuz'mina, G. G. Aleksandrov, “Synthesis and structures of complexes ofN-(2-aminoethyl)diaziridines with transition metal salts”, Russ Chem Bull, 49:11 (2000), 1882
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