Abstract:
Crystal structure of widely employed precatalyst [Pd(Ph3P)4] is reported. It crystallizes in P-3 space group [a = 19.0828(8) and c = 26.4423(18) Å] with six molecules per unit cell. It is demonstrated that the phase purity of this important compound can now be routinely controlled via powder X-ray diffraction analysis.
Citation:
T. S. Sukhikh, M. P. Davydova, A. V. Artem’ev, “Crystal structure of tetrakis(triphenylphosphine)palladium(0)”, Mendeleev Commun., 33:2 (2023), 171–173
Linking options:
https://www.mathnet.ru/eng/mendc340
https://www.mathnet.ru/eng/mendc/v33/i2/p171
This publication is cited in the following 4 articles:
A. Yu. Baranov, I. Yu. Bagryanskaya, A. V. Artem'ev, Mendeleev Commun., 35:1 (2025), 39–41
Pavel V. Nikulshin, Alexander Yu. Makarov, Igor P. Koskin, Christina S. Becker, Maxim S. Kazantsev, Jens Beckmann, Yaser Balmohammadi, Simon Grabowsky, Stefan Mebs, Olga V. Naumova, Dmitry Yu. Protasov, Kirill A. Svit, Irina G. Irtegova, Ekaterina A. Radiush, Irina Yu. Bagryanskaya, Leonid A. Shundrin, Andrey V. Zibarev, “1,2,3,4‐Tetrafluorobiphenylene: A Prototype Janus‐Headed Scaffold for Ambipolar Materials”, ChemPlusChem, 89:5 (2024)
Yu. N. Kononevich, A. D. Volodin, A. A. Korlyukov, V. K. Brel, A. M. Muzafarov, “A new efficient synthesis of Pyrphos ligand”, Mendeleev Commun., 34:1 (2024), 51–53
M. P. Davydova, T. S. Sukhikh, A. V. Artem'ev, “Tris[(pyridin-4-yl)methyl]phosphine, its P-oxide and CuI-based 1D polymer thereof”, Mendeleev Commun., 34:3 (2024), 345–347
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