R. G. Kostyanovsky, V. G. Shtamburg, O. V. Shishkin, R. I. Zubatyuk, V. V. Shtamburg, A. A. Anishchenko, A. V. Mazepa, “Pyramidal nitrogen in the crystal of N-[(benzoyl)-(hydroxy)methyl]-N-benzyloxy-N’-(2-bromophenyl)urea”, Mendeleev Commun., 20:3 (2010), 167

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Mendeleev Communications, 2010, Volume 20, Issue 3, Pages 167–169
DOI: https://doi.org/10.1016/j.mencom.2010.05.015 (Mi mendc3026)

This article is cited in 6 scientific papers (total in 6 papers)

Pyramidal nitrogen in the crystal of N-[(benzoyl)-(hydroxy)methyl]-N-benzyloxy-N’-(2-bromophenyl)urea

R. G. Kostyanovsky^a, V. G. Shtamburg^b, O. V. Shishkin^c, R. I. Zubatyuk^c, V. V. Shtamburg^d, A. A. Anishchenko^d, A. V. Mazepa^e

^a N.N. Semenov Federal Research Center for Chemical Physics, Russian Academy of Sciences, Moscow, Russian Federation
^b Ukrainian State University of Chemical Technology, Dnepropetrovsk, Ukraine
^c STC 'Institute for Single Crystals', National Academy of Sciences of Ukraine, Kharkov, Ukraine
^d Department of Chemistry, Dnepropetrovsk National University, Dnepropetrovsk, Ukraine
^e A.V. Bogatsky Physico-Chemical Institute, National Academy of Sciences of Ukraine, Odessa, Ukraine

Full-text PDF (473 kB) Citations (6)

DOI: https://doi.org/10.1016/j.mencom.2010.05.015

Abstract: Phenylglyoxal reacts with N-benzyloxy-N’-(2-bromophenyl)urea forming N-[(benzoyl)(hydroxy)methyl]-N-benzyloxy-N’-(2-bromophenyl)urea. As it was found by XRD study, the molecules of the latter in crystal exist in two forms which vary in a different degree of pyramidality of the same nitrogen atom. Reactions of N-ethoxy-N’-phenylurea and N-benzyloxy-N’-(4-nitrophenyl) urea with phenylglyoxal lead to cyclic products.

Document Type: Article

Language: English

Citation: R. G. Kostyanovsky, V. G. Shtamburg, O. V. Shishkin, R. I. Zubatyuk, V. V. Shtamburg, A. A. Anishchenko, A. V. Mazepa, “Pyramidal nitrogen in the crystal of N-[(benzoyl)-(hydroxy)methyl]-N-benzyloxy-N’-(2-bromophenyl)urea”, Mendeleev Commun., 20:3 (2010), 167–169

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https://www.mathnet.ru/eng/mendc3026

https://www.mathnet.ru/eng/mendc/v20/i3/p167

This publication is cited in the following 6 articles:

Vasiliy G. Shtamburg, Victor V. Shtamburg, Andrey A. Anishchenko, Alexander V. Mazepa, Eduard B. Rusanov, “3-Alkoxy-1,5-bis(aryl)imidazolidine-2,4-diones, synthesis and structure”, Journal of Molecular Structure, 1264 (2022), 133259
Vasiliy G. Shtamburg, Victor V. Shtamburg, Andrey A. Anishchenko, Alexander V. Mazepa, Eduard B. Rusanov, “Interaction of Ninhydrin with N-Alkoxy-N'-arylureas and N-Alkoxy-N'-alkylureas. 1-Alkoxy-3-aryl(alkyl)-3a,8a-dihydroxy-1,3,3a,8a-tetrahydroindeno [1,2-d]imidazole-2,8-diones: Synthesis and Structure”, Journal of Molecular Structure, 1248 (2022), 131443
Jacobus A. W. Jong, Robert Smakman, Marc-Etienne Moret, Marianne C. Verhaar, Wim E. Hennink, Karin G. F. Gerritsen, Cornelus F. Van Nostrum, “Reactivity of (Vicinal) Carbonyl Compounds with Urea”, ACS Omega, 4:7 (2019), 11928
Vasiliy G. Shtamburg, Viktor V. Shtamburg, Andrey A. Anishchenko, Roman I. Zubatyuk, Aleksander V. Mazepa, Eugene A. Klotz, Svetlana V. Kravchenko, Remir G. Kostyanovsky, “Single-stage synthesis of 3-hydroxy- and 3-alkoxy-5-arylimidazolidine-2,4-diones by reaction of arylglyoxal hydrates with N-hydroxy- and N-alkoxyureas”, Chem Heterocycl Comp, 51:6 (2015), 553
Gihaeng Kang, Jineun Kim, Eunjin Kwon, Tae Ho Kim, “Crystal structure of metobromuron”, Acta Crystallogr E Cryst Commun, 71:8 (2015), o589
Bagher Eftekhari-Sis, Maryam Zirak, Ali Akbari, “Arylglyoxals in Synthesis of Heterocyclic Compounds”, Chem. Rev., 113:5 (2013), 2958

Citing articles in Google Scholar: Russian citations, English citations
Related articles in Google Scholar: Russian articles, English articles

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