N. B. Tamm, V. Yu. Markov, S. I. Troyanov, “Synthesis, HPLC isolation and structural characterization of three new C60(CF3)18 isomers”, Mendeleev Commun., 35:2 (2025), 130

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Mendeleev Communications, 2025, Volume 35, Issue 2, Pages 130–132
DOI: https://doi.org/10.71267/mencom.7634 (Mi mendc1380)

Communications

Synthesis, HPLC isolation and structural characterization of three new C₆₀(CF₃)₁₈ isomers

N. B. Tamm, V. Yu. Markov, S. I. Troyanov

Department of Chemistry, M. V. Lomonosov Moscow State University, 119991 Moscow, Russian Federation

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DOI: https://doi.org/10.71267/mencom.7634

Graphic abstract: Synthesis, HPLC isolation and structural characterization of three new C<sub>60</sub>(CF<sub>3</sub>)<sub>18</sub> isomers

Abstract: Three new C₆₀(CF₃)₁₈ isomers have been synthesized by high-temperature trifluoromethylation of [60]fullerene with gaseous CF₃I, isolated by HPLC, and structurally characterized by single crystal X-ray diffraction using synchrotron radiation.

Keywords: fullerene C₆₀, trifluoromethylation, HPLC separation, synchrotron radiation, structure elucidation.

Funding agency	Grant number
Chemical thermodynamics and theoretical material science	21031300039-1

Received: 01.10.2024
Accepted: 12.11.2024

Document Type: Article

Language: English

Citation: N. B. Tamm, V. Yu. Markov, S. I. Troyanov, “Synthesis, HPLC isolation and structural characterization of three new C₆₀(CF₃)₁₈ isomers”, Mendeleev Commun., 35:2 (2025), 130–132

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