Abstract:
New aspects of multicomponent condensation reactions of ethylene/propylenediamine, formaldehyde and unsubstituted and 1-methyl substituted semithio- and dithioglycolurils have been examined. Ethylene-linked 2,3a,4a,6,9,10a,11aheptaaza-6,9-methanobenzo[cd]cyclonona[gh]pentalene and 2,6:10,14-dimethano-2,6,7a,8a,10,14,15a,16a-octaazadicyclodeca[cd,gh]pentalene as well as their simpler analogues were synthesized, and their structures were proved by 1D and 2D NMR spectroscopy, HRMS and X-ray analysis.
Citation:
V. V. Baranov, Ya. A. Barsegyan, Yu. A. Strelenko, V. A. Karnoukhova, A. N. Kravchenko, “New cage-fused polyaza polycyclic systems based on thioglycolurils and alkanediamines”, Mendeleev Commun., 30:4 (2020), 479–481
Linking options:
https://www.mathnet.ru/eng/mendc1229
https://www.mathnet.ru/eng/mendc/v30/i4/p479
This publication is cited in the following 6 articles:
Anton A. Galochkin, Vladimir V. Baranov, Karl A. Hansford, Louise I. M. Friberg, Elena D. Strel'tzova, Egor S. Lipatov, Yulia V. Nelyubina, Angelina N. Kravchenko, “Synthesis, Structures and Antifungal Activity of Selenoglycolurils”, ChemistrySelect, 8:14 (2023)
Cheng Geng, “Modelling of mixed thermodynamic model based on new materials”, Therm sci, 27:2 Part A (2023), 1067
V. V. Baranov, T. N. Vol'khina, N. G. Kolotyrkina, A. N. Kravchenko, “Synthesis and crystal structures of novel glycoluril carboxylic acids conglomerates”, Mendeleev Commun., 32:4 (2022), 537–539
A. A. Galochkin, V. V. Baranov, N. G. Kolotyrkina, A. N. Kravchenko, “Synthesis of trialkyl semithioglycolurils from alkylthiourea-glyoxal cyclic adducts and dialkylureas”, Mendeleev Commun., 32:6 (2022), 771–773
Elena A. Mamaeva, Anastasiya V. Leppa, Abdigali A. Bakibayev, “Selective synthesis of a novel glycoluril-based hybrid compound with high application potential”, Chem Heterocycl Comp, 57:6 (2021), 700
I. Yu. Titov, V. S. Stroylov, P. V. Rusina, I. Svitanko, “Preliminary modelling as the first stage of targeted organic synthesis”, Russian Chem. Reviews, 90:7 (2021), 831–867